The TGA body weight improve curve is shown in Determine 1. The primary weight loss phase could be the volatilization accompanied by An important decomposition move. The by-product of weight adjust curve in eco-friendly reveals a peak in which the height max is at 427.71 ˚C. The MS knowledge is collected all through the entire TGA experiment. Ion currents and TGA mass decline are plotted like a purpose of temperature (see Figure 2). It is important to bear in mind the goods of a TGA take a look at are normally decomposition merchandise, and that is real in these experiments also. Thus, the aim is to comprehend the thermal degradation products and solutions of nylon 66. TGA-MS repeatedly displays the decomposition off gases as being a operate of your time and temperature. The degradation system from the polymer molecules breaking with the C-N bond results in lesser polymer molecules Using the very same device of bicarbonyl polymethylene fragments and also the fragments will break down into carbon dioxide, carbon monoxide, drinking water, and hydrocarbons [five].

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The degradation of nylon 66 On this Portion of the research was also performed with a TGA5500. The off-fuel merchandise have been analyzed utilizing a FTIR to the IR spectra as well as a GC/MS for the MS Evaluation.

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The TGA-FTIR effects compliment the TGA-MS final results. Each techniques provide practical information regarding the constructions in the off-gas products from your nylon 66 thermal degradation course of action. FTIR can be quite helpful to establish the presence of certain chemical bonds and many practical teams in polymers. It is actually commonly utilized for polymer characterization.